Ultra Preconcentration of Polycyclic Aromatic Hydrocarbons in Smoked Bacon by a Combination of SPE and DLLME

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Ultra preconcentration of polycyclic aromatic hydrocarbons in smoked bacon by a combination of SPE and DLLME.

A sample pretreatment method, solid-phase extraction combined with dispersive liquid-liquid microextraction (SPE-DLLME), was established for the sensitive determination of polycyclic aromatic hydrocarbons (PAHs) in smoked bacon samples. In the SPE-DLLME process, three PAHs including naphthalene (Naph), phenanthrene (Phen) and pyrene (Pyr) were extracted from samples and transferred into C18 SPE...

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Polycyclic aromatic hydrocarbons in smoked cheese

BACKGROUND: Polycyclic aromatic hydrocarbons (PAHs) represent a group of organic compounds containing two or more aromatic rings. Their control in the human food chain is required due to the mutagenic and carcinogenic potential, exhibited in vertebrates. In the present study, the occurrence of PAHs in 36 cheeses smoked by various processes was investigated. RESULTS: PAH concentrations (sum of 1...

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Transport of Polycyclic Aromatic Hydrocarbons in a Calcareous Wetland Soil

Knowledge of transport and degradation of polycyclic aromatic hydrocarbons (PAHs) is important in assessing PAH contamination of soils and water resources. The transport of naphthalene, anthracene, pyrene and phenanthrene was determined in a contaminated calcareous soil obtained from the Shadegan wetland (Khozestan, Iran) considering a column study in laboratory conditions. The PAHs were added ...

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Determination of Some Polycyclic Aromatic Hydrocarbons in the Caspian Seawater by HPLC Following Preconcentration with Solid-Phase Extraction

A solid-phase extraction (SPE) method for sample clean-up and preconcentration followed by reversed-phase high-performance liquid chromatography (RP-HPLC) with uv detection is reported for determination of polycyclic aromatic hydrocarbons (PAHs) in the caspian seawater. A good resolution was obtained using acetonitrile:water (40:60) as mobile-phase for separation of these compounds. The eff...

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Biodegradation of polycyclic aromatic hydrocarbons, toxic compounds widely distributed in the environment by bacteria, is a cheap and safe cleaning up method. The present study attempts to isolate and characterize dioxygenase-producing bacteria which are able to degrade phenanthrene and pyrene from refinery soils. It also aims to assess in vitro biodegradation. To do so, two contaminated soil s...

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ژورنال

عنوان ژورنال: Journal of Chromatographic Science

سال: 2013

ISSN: 0021-9665,1945-239X

DOI: 10.1093/chromsci/bmt119